Thiophosphation of 2-methyl-2-nitro-1-propanol and the preparation of monothiophosphoric acid
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Thiophosphation of 2-methyl-2-nitro-1-propanol and the preparation of monothiophosphoric acid
The thiophosphation of a ni troalcohol was studied in ether and in p yridine so lu tion. ,rhen 2-methyl-2-nitro-l-propanol was r eftuxed wi th phosphorus pentasulfide in ether , t he corresponding dithiophosphate was form ed . In p yridine so lu t ion , however, a pyridine sal t of th e secondary di t hiophosphate was formed. A pyridine sal t of meta t rithophosphoric a cid was also isolated fr...
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ژورنال
عنوان ژورنال: Journal of Research of the National Bureau of Standards
سال: 1952
ISSN: 0091-0635
DOI: 10.6028/jres.048.040